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In the present study a series of metal complex of [bis (2-amino-5-aryl-1,3,4-thiadiazole]2Cl (S1-S9) was synthesized by using ultrasound irradiation technique. The metal complex was synthesized by the reaction between ligand and appropriate metal salts (CuCl2. 2H2O, CoCl2. 6H₂O, ZnCl₂, MgCl₂. 4H₂O, NiCl₂. 6H₂O). Significant activity was observed for synthesized metal complexes S6 and S7 against B. subtilis and S. aureus.