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ABSTRACT

The present investigation describes the geometry of an original compound, Titanium (IV) molybdotungstate [TiMoW] prepared by using the ion-exchange route. To elaborate the structural aspects various analytical techniques were employed. The amorphous behavior of the compound was established using XRD. Infrared spectroscopy was used to assign dynamic sites responsible for acidic characteristics of the sample. SEM/EDS has been used to describe the composition of elements present in the prepared sample. Thermogravimetric techniques indicated the weight loss rate and helped in ascertaining the number of water molecules. Thereafter, the derived structure furnished a geometry of heteropolyacid salt, embedded with acidic and ion exchange characteristics.

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